WO2002072471A3 - Verfahren zur herstellung von multinären metalloxidpulvern in einem pulsationsreaktor - Google Patents

Verfahren zur herstellung von multinären metalloxidpulvern in einem pulsationsreaktor Download PDF

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Publication number
WO2002072471A3
WO2002072471A3 PCT/EP2002/002408 EP0202408W WO02072471A3 WO 2002072471 A3 WO2002072471 A3 WO 2002072471A3 EP 0202408 W EP0202408 W EP 0202408W WO 02072471 A3 WO02072471 A3 WO 02072471A3
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WIPO (PCT)
Prior art keywords
metal oxide
producing
oxide powders
multinary metal
pulsed reactor
Prior art date
Application number
PCT/EP2002/002408
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English (en)
French (fr)
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WO2002072471A2 (de
Inventor
Stefan Remke
Bernd Mueller
Guenter Riedel
Stefan Ambrosius
Bernd Dahm
Original Assignee
Merck Patent Gmbh
Stefan Remke
Bernd Mueller
Guenter Riedel
Stefan Ambrosius
Bernd Dahm
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Merck Patent Gmbh, Stefan Remke, Bernd Mueller, Guenter Riedel, Stefan Ambrosius, Bernd Dahm filed Critical Merck Patent Gmbh
Priority to AT02729963T priority Critical patent/ATE490216T1/de
Priority to JP2002571398A priority patent/JP2004526653A/ja
Priority to KR10-2003-7011845A priority patent/KR20040012731A/ko
Priority to US10/471,590 priority patent/US7358212B2/en
Priority to CA002440613A priority patent/CA2440613A1/en
Priority to AU2002302391A priority patent/AU2002302391A1/en
Priority to EP02729963A priority patent/EP1370486B1/de
Priority to DE50214795T priority patent/DE50214795D1/de
Publication of WO2002072471A2 publication Critical patent/WO2002072471A2/de
Publication of WO2002072471A3 publication Critical patent/WO2002072471A3/de

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    • C01B13/00Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/14Methods for preparing oxides or hydroxides in general
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
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    • B01J19/24Stationary reactors without moving elements inside
    • B01J19/241Stationary reactors without moving elements inside of the pulsating type
    • BPERFORMING OPERATIONS; TRANSPORTING
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    • B01J6/00Heat treatments such as Calcining; Fusing ; Pyrolysis
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Abstract

Die Erfindung betrifft ein Verfahren zur Herstellung eines einteiligen, multinären Metalloxidpulvers, das zur Herstellung von Hochtemperatur-Supraleitern geeignet ist. Hierzu wir ein Gemisch der entsprechenden Metallsalze und/oder Metalloxide und/oder Metalle im erforderlichen stöchiometrischen Verhältnis in einen Pulsationsreaktor mit einer pulsierenden, aus einer flammenlosen Verbrennung resultierenden Gasströmung eingebracht und teilweise oder vollständig zum multinären Metalloxid umgesetzt.
PCT/EP2002/002408 2001-03-13 2002-03-06 Verfahren zur herstellung von multinären metalloxidpulvern in einem pulsationsreaktor WO2002072471A2 (de)

Priority Applications (8)

Application Number Priority Date Filing Date Title
AT02729963T ATE490216T1 (de) 2001-03-13 2002-03-06 Verfahren zur herstellung von multinären metalloxidpulvern in einem pulsationsreaktor
JP2002571398A JP2004526653A (ja) 2001-03-13 2002-03-06 複数の金属酸化物粉末のパルスリアクタでの製造方法
KR10-2003-7011845A KR20040012731A (ko) 2001-03-13 2002-03-06 맥동 반응기에서의 다원성 금속 산화물 분말의 제조 방법
US10/471,590 US7358212B2 (en) 2001-03-13 2002-03-06 Method for producing multinary metal oxide powders in a pulsed reactor
CA002440613A CA2440613A1 (en) 2001-03-13 2002-03-06 Method for producing multinary metal oxide powders in a pulsed reactor
AU2002302391A AU2002302391A1 (en) 2001-03-13 2002-03-06 Method for producing multinary metal oxide powders in a pulsed reactor
EP02729963A EP1370486B1 (de) 2001-03-13 2002-03-06 Verfahren zur herstellung von multinären metalloxidpulvern in einem pulsationsreaktor
DE50214795T DE50214795D1 (de) 2001-03-13 2002-03-06 Verfahren zur herstellung von multinären metalloxidpulvern in einem pulsationsreaktor

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10111938A DE10111938A1 (de) 2001-03-13 2001-03-13 Herstellung von Hochtemperatur-Supraleiter-Pulvern in einem Pulsationsreaktor
DE10111938.0 2001-03-13

Publications (2)

Publication Number Publication Date
WO2002072471A2 WO2002072471A2 (de) 2002-09-19
WO2002072471A3 true WO2002072471A3 (de) 2003-10-02

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US (1) US7358212B2 (de)
EP (1) EP1370486B1 (de)
JP (1) JP2004526653A (de)
KR (1) KR20040012731A (de)
CN (1) CN1257100C (de)
AT (1) ATE490216T1 (de)
AU (1) AU2002302391A1 (de)
CA (1) CA2440613A1 (de)
DE (2) DE10111938A1 (de)
WO (1) WO2002072471A2 (de)

Families Citing this family (50)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20010036437A1 (en) * 2000-04-03 2001-11-01 Andreas Gutsch Nanoscale pyrogenic oxides
AU2003253400A1 (en) * 2002-12-23 2004-07-22 Universitat Tubingen Method for the production of nitrate-containing precursors for metal oxides and oxocuptrate superconductors
US7589046B2 (en) * 2003-06-04 2009-09-15 Basf Aktiengesellschaft Thermal treatment of the precursor material of a catalytically active material
DE10328342B4 (de) * 2003-06-24 2006-05-04 Graphit Kropfmühl AG Verfahren zur Herstellung von expandiertem Graphit, expandierter Graphit und Verwendung
DE102004041747A1 (de) * 2004-08-28 2006-03-02 Degussa Ag Indium-Zinn-Mischoxidpulver
DE102004044266A1 (de) * 2004-09-10 2006-03-30 Umicore Ag & Co. Kg Verfahren zur Herstellung alkalimetallhaltiger, mehrkomponentiger Metalloxidverbindungen und damit hergestellte Metalloxidverbindungen
CN100372596C (zh) * 2005-01-13 2008-03-05 清华大学 一种燃煤排放可吸入颗粒物及其前驱体的脱除方法及装置
DE102005002659A1 (de) * 2005-01-19 2006-07-27 Merck Patent Gmbh Verfahren zur Herstellung von Mischoxiden mittels Sprühpyrolyse
JP4799885B2 (ja) * 2005-03-14 2011-10-26 株式会社 赤見製作所 金属化合物粉末の製造法
DE102005061897A1 (de) * 2005-12-23 2007-06-28 Degussa Gmbh Verfahren zur Herstellung von pulverförmigen Feststoffen
JP5226658B2 (ja) * 2006-03-10 2013-07-03 カウンスィル オブ サイエンティフィック アンド インダストリアル リサーチ 向上した特性を有する高温超電導バルク体電流リードの製造方法及びそれによってつくられる超電導バルク体電流リード
JP5034314B2 (ja) * 2006-05-19 2012-09-26 住友大阪セメント株式会社 高屈折率透明粒子の製造方法と高屈折率透明粒子及び高屈折率透明複合体並びに発光素子
DE102006027133A1 (de) * 2006-06-12 2007-12-13 Merck Patent Gmbh Verfahren zur Herstellung von Granat-Leuchtstoffen in einem Pulsationsreaktor
DE102006027334A1 (de) * 2006-06-13 2008-01-10 Evonik Degussa Gmbh Verfahren zur Herstellung von Metalloxidpulvern
DE102006046806B4 (de) * 2006-06-14 2008-10-30 Ibu-Tec Advanced Materials Gmbh Verfahren zur Herstellung von beschichteten Partikeln und Verwendung eines thermischen Reaktors zur Durchführung des Verfahrens
DE102006032452B4 (de) * 2006-07-13 2013-10-02 Süd-Chemie Ip Gmbh & Co. Kg Verfahren zur Herstellung nanokristalliner Metalloxide
DE102006039462B4 (de) * 2006-08-23 2010-02-18 Ibu-Tec Advanced Materials Ag Verfahren zur Herstellung von Partikeln
CN101511730B (zh) * 2006-09-07 2012-05-09 Sued-化学公司 制备纳米晶体混合金属氧化物的方法及由该方法获得的纳米晶体混合金属氧化物
DE102006046803A1 (de) * 2006-09-29 2008-04-03 Ibu-Tec Gmbh & Co. Kg Verfahren und thermischer Reaktor zur Herstellung von Partikeln
DE102007003744A1 (de) 2007-01-19 2008-07-31 Ibu-Tec Advanced Materials Gmbh Verfahren und thermischer Reaktor zur Herstellung von Partikeln
DE102007059990A1 (de) 2007-12-13 2009-06-18 Süd-Chemie AG Verfahren zur Herstellung nanokristalliner Hydrotalcitverbindungen
DE102008006607B4 (de) 2008-01-30 2011-03-03 Ibu-Tec Advanced Materials Ag Verfahren zur Herstellung feinteiliger Partikel
DE102008017308B4 (de) * 2008-04-04 2014-09-25 Süd-Chemie Ip Gmbh & Co. Kg Verfahren zur Herstellung von nanokristallinen Bismut-Molybdänmischoxidkatalysatoren
DE102008020600B4 (de) * 2008-04-24 2010-11-18 Outotec Oyj Verfahren und Anlage zur Wärmebehandlung feinkörniger mineralischer Feststoffe
JP2011096394A (ja) * 2009-10-27 2011-05-12 Univ Of Fukui リチウムイオン二次電池正極活物質の製造方法
JP5289511B2 (ja) * 2011-06-24 2013-09-11 株式会社 赤見製作所 金属化合物粉末の製造法
CN103896576A (zh) * 2014-03-06 2014-07-02 北京英纳超导技术有限公司 一种改性铋系超导粉及其制备方法
EP2982435A1 (de) 2014-08-07 2016-02-10 Kronos International, Inc. Verfahren zur Herstellung eines kohlenstoffhaltigen Photokatalysators auf Basis von Titandioxid
CN104445356B (zh) * 2014-10-30 2016-06-29 东南大学 含铜金属复合氧化物光催化材料的制备方法
EP3053571B1 (de) 2015-02-05 2017-03-22 Dentsply DeTrey GmbH Verfahren zur Herstellung einer teilchenförmigen Dentalfüllstoffzusammensetzung
DE102015003398B4 (de) 2015-03-18 2018-11-22 Dennert Poraver Gmbh Verfahren und Anlage zur Herstellung von Mikrohohlkugeln aus Glas und Verwendung eines Pulsationsreaktors
CN106986560A (zh) * 2016-01-20 2017-07-28 海城市后英经贸集团有限公司 一种垱设脉冲燃烧设施
DE102017126363A1 (de) * 2017-11-10 2019-05-16 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Vorrichtung und Verfahren zur Herstellung eines Zeoliths
DE102017126365A1 (de) * 2017-11-10 2019-05-16 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Vorrichtung und Verfahren zur Herstellung eines Zeoliths
DE102017128734A1 (de) 2017-12-04 2019-06-06 Schott Ag Verbundmaterial, umfassend wenigstens ein erstes Material und Partikel, wobei die Partikel einen negativen thermischen Ausdehnungskoeffizienten α aufweisen, und Klebematerial umfassend das Verbundmaterial
DE102017128719A1 (de) 2017-12-04 2019-06-06 Schott Ag Lithiumionenleitendes Verbundmaterial, umfassend wenigstens ein Polymer und lithiumionenleitende Partikel, und Verfahren zur Herstellung eines Lithiumionenleiters aus dem Verbundmaterial
DE102018211650A1 (de) 2018-07-12 2020-01-16 Ibu-Tec Advanced Materials Ag Vorrichtung zur Herstellung von Partikeln
DE102018211639A1 (de) 2018-07-12 2020-01-16 Ibu-Tec Advanced Materials Ag Vorrichtung und Verfahren zur Herstellung von Partikeln
DE102018211652A1 (de) 2018-07-12 2020-01-16 Ibu-Tec Advanced Materials Ag Vorrichtung zur Herstellung von Partikeln
DE102018211628A1 (de) 2018-07-12 2020-01-16 Ibu-Tec Advanced Materials Ag Vorrichtung zur Herstellung von Partikeln
DE102018211645A1 (de) * 2018-07-12 2020-01-16 Ibu-Tec Advanced Materials Ag Vorrichtung zur Herstellung von Partikeln
DE102018211641A1 (de) 2018-07-12 2020-01-16 Ibu-Tec Advanced Materials Ag Vorrichtung und Verfahren zur Herstellung von Partikeln
DE102018211635A1 (de) 2018-07-12 2020-01-16 Ibu-Tec Advanced Materials Ag Vorrichtung zur Herstellung von Partikeln
DE102019210282A1 (de) 2018-07-12 2020-01-16 Ibu-Tec Advanced Materials Ag Vorrichtung zur Herstellung von Partikeln
CN109244229B (zh) * 2018-09-13 2022-03-18 安徽建筑大学 一种微电子超导材料及其制备方法
DE102019206727A1 (de) 2019-05-09 2020-11-12 Ibu-Tec Advanced Materials Ag Vorrichtung zur thermischen Behandlung eines Rohstoffs in einem pulsierenden Heißgasstrom
DE102019218690A1 (de) * 2019-12-02 2021-06-02 Ibu-Tec Advanced Materials Ag Vorrichtung zur Herstellung von Partikeln
WO2021175849A1 (de) 2020-03-02 2021-09-10 Ibu-Tec Advanced Materials Ag Verfahren zur thermischen behandlung eines batteriematerials in einem thermischen reaktor
EP4327927A1 (de) 2022-08-23 2024-02-28 IBU-tec advanced materials AG Verfahren und reaktor zur thermischen behandlung von batterievorläufermaterial
CN115414962B (zh) * 2022-09-22 2023-09-15 西北有色金属研究院 一种制备分子筛负载多元合金纳米颗粒材料的方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19608841C1 (de) * 1996-03-07 1997-08-28 Heidelberger Zement Ag Verfahren zur Herstellung von Metakaolin aus kaolinitischem Ton
DE19614430C1 (de) * 1996-04-12 1997-10-02 Pfeifer & Langen Verfahren zur Herstellung von Calciumoxid aus gefälltem Calciumcarbonat und Verwendungen
EP0905104A1 (de) * 1997-09-25 1999-03-31 Aventis Research & Technologies GmbH & Co. KG Verfahren zur Herstellung von hochtemperatursupraleitenden Bi (Pb) SrCaCuO-haltigen Pulvern und deren Verwendung
WO1999038819A1 (de) * 1998-01-30 1999-08-05 Aventis Research & Technologies Gmbh & Co. Kg Verfahren zum herstellen von oxidischen pulvers mit geringen kohlenstoff- und wasserstoffgehalten, deren verwendung sowie mischoxide für hochtemperatursupraleiter und hochtemperatursupraleiter

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2606698B2 (ja) * 1987-03-23 1997-05-07 株式会社 半導体エネルギー研究所 超電導セラミツクスの作製方法
JP2630361B2 (ja) * 1987-03-27 1997-07-16 株式会社 半導体エネルギー研究所 超電導材料
JPH0649626B2 (ja) * 1987-08-27 1994-06-29 株式会社半導体エネルギ−研究所 酸化物超電導材料
US5106830A (en) * 1988-01-15 1992-04-21 University Of Arkansas High temperature superconductor system having the formula Tl-Ba-Cu-O
US5340796A (en) * 1988-02-12 1994-08-23 At&T Bell Laboratories Oxide superconductor comprising Cu, Bi, Ca and Sr
CA1341504C (en) * 1988-03-25 2006-04-11 Jun Akimitsu Substituted superconductive bi-sr-ca-cu oxide and bi-sr-ca-ln-cu oxide compositions
US5114702A (en) * 1988-08-30 1992-05-19 Battelle Memorial Institute Method of making metal oxide ceramic powders by using a combustible amino acid compound
US5348935A (en) * 1988-10-28 1994-09-20 The Regents Of The University Of California Highly oxidized superconductors
US4997808A (en) * 1988-12-27 1991-03-05 Eastman Kodak Company Superconductive ceramic oxide combination
US5306697A (en) * 1989-02-10 1994-04-26 University Of Houston - University Park Oriented grained Y-Ba-Cu-O superconductors having high critical currents and method for producing same
JP3205997B2 (ja) * 1990-09-21 2001-09-04 東レ株式会社 超電導体
US5204313A (en) * 1990-12-07 1993-04-20 Eastman Kodak Company Process of forming a high temperature superconductor on a metal substrate surface
GB9409660D0 (en) * 1994-05-13 1994-07-06 Merck Patent Gmbh Process for the preparation of multi-element metaloxide powders
US6027826A (en) * 1994-06-16 2000-02-22 The United States Of America As Represented By The Secretary Of The Air Force Method for making ceramic-metal composites and the resulting composites
JPH0881221A (ja) * 1994-09-13 1996-03-26 Furukawa Electric Co Ltd:The 酸化物超電導体およびその製造方法
US5919735A (en) * 1994-11-04 1999-07-06 Agency Of Industrial Science And Technology High temperature superconductor
US6540838B2 (en) * 2000-11-29 2003-04-01 Genus, Inc. Apparatus and concept for minimizing parasitic chemical vapor deposition during atomic layer deposition
US6200893B1 (en) * 1999-03-11 2001-03-13 Genus, Inc Radical-assisted sequential CVD
US6677278B1 (en) * 1999-07-30 2004-01-13 Merck Patent Gmbh Pb-Bi-Sr-Ca-Cu-oxide powder mix with enhanced reactivity and process for its manufacture
US6794339B2 (en) * 2001-09-12 2004-09-21 Brookhaven Science Associates Synthesis of YBa2CU3O7 using sub-atmospheric processing
KR100460841B1 (ko) * 2002-10-22 2004-12-09 한국전자통신연구원 플라즈마 인가 원자층 증착법을 통한 질소첨가 산화물박막의 형성방법

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19608841C1 (de) * 1996-03-07 1997-08-28 Heidelberger Zement Ag Verfahren zur Herstellung von Metakaolin aus kaolinitischem Ton
DE19614430C1 (de) * 1996-04-12 1997-10-02 Pfeifer & Langen Verfahren zur Herstellung von Calciumoxid aus gefälltem Calciumcarbonat und Verwendungen
EP0905104A1 (de) * 1997-09-25 1999-03-31 Aventis Research & Technologies GmbH & Co. KG Verfahren zur Herstellung von hochtemperatursupraleitenden Bi (Pb) SrCaCuO-haltigen Pulvern und deren Verwendung
WO1999038819A1 (de) * 1998-01-30 1999-08-05 Aventis Research & Technologies Gmbh & Co. Kg Verfahren zum herstellen von oxidischen pulvers mit geringen kohlenstoff- und wasserstoffgehalten, deren verwendung sowie mischoxide für hochtemperatursupraleiter und hochtemperatursupraleiter

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
SHELUKAR S.D. ET AL: "Continuous Rotary Kiln Calcination of YBaCuO Precursor Powders", IND. ENG. CHEM. RES., vol. 33, 1994, pages 421 - 427, XP002239301 *

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